This protocol describes the detailed procedure for preparation of DADS-nFeS. To get our target nanoparticle with stable property, we synthesised DADS-nFeS by solvothermal method with high temperatures and pressures.
Method Article
Protocol for synthesis of DADS-nFeS
https://doi.org/10.1038/protex.2018.138
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This protocol has been posted on Protocol Exchange, an open repository of community-contributed protocols sponsored by Nature Portfolio. These protocols are posted directly on the Protocol Exchange by authors and are made freely available to the scientific community for use and comment.
posted 03 Dec, 2018
You are reading this latest protocol version
This protocol describes the detailed procedure for preparation of DADS-nFeS. To get our target nanoparticle with stable property, we synthesised DADS-nFeS by solvothermal method with high temperatures and pressures.
This protocol describes the detailed procedure for preparation of DADS-nFeS. We synthesized DADS-nFeS by solvothermal method under high temperature and pressure in a sealed autoclave reactor.
ethylene glycol, FeCl3•6H2O, sodium acetate(NaOAc), diallyl sulfide(DADS)
magnetic stirring bar, oven, Teflon-lined stainless steel autoclave
14 h or longer (including the mixing process and the reaction time under high temperature and high pressure)
The new formed products are black (or brown if the drying process is much more sufficent) powder which consist of hexagonal sheet-like nanostructures and sphere nanoparticles under the electron microscope.
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3.Fan, K. et al. Optimization of Fe3O4 nanozyme activity via single amino acid modification mimicking an enzyme active site.Chem Commun 53, 424-427(2016).
The authors declare no conflicting financial interests.
This protocol has been posted on Protocol Exchange, an open repository of community-contributed protocols sponsored by Nature Portfolio. These protocols are posted directly on the Protocol Exchange by authors and are made freely available to the scientific community for use and comment.
posted 03 Dec, 2018
You are reading this latest protocol version
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