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Method Article
Synthesis of 1,3–bis(2,4,6–trimethylphenyl)–imidazolinium salts : SIMes.HCl, SIMes.HBr, SIMes.HBF4 and SIMes.HPF6.
Arnaud Gautier
CNRS
Corresponding Author
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N,N’–bis–(2,4,6–trimethylphenylamino)ethane dihydrobromide is obtained in a single step through the dialkylation of dibromoethane. It serves as a versatile starting material for the synthesis of imidazolium salts: SIMes.HBr, SIMes.HCl, SIMes.HPF6 and SIMes.HBF4.
Keywords
imidazolinium salts, NHC precursors, diamines
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Associated Publications
Synthesis of 1,2 diamines under environmentally benign conditions: application for the preparation of imidazolidiniums
by Stéphane P. Roche, Marie-Laure Teyssot, and Arnaud Gautier
Tetrahedron Letters (27 September, 2012)
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This is a preprint. It has not completed peer review.
Method Article
Synthesis of 1,3–bis(2,4,6–trimethylphenyl)–imidazolinium salts : SIMes.HCl, SIMes.HBr, SIMes.HBF4 and SIMes.HPF6.
Arnaud Gautier
CNRS
Corresponding Author
Badges
Prescreen
This manuscript passed our Prescreen assessment
Complete author information
Appropriate declaration statements
Potential risks to human health
Prescreen
History
CURRENT STATUS: Posted
Version 1
Posted 10 Oct, 2012
No community comments so far
Metrics
Comments: 0
HTML Views: ...
Subject Areas
Synthetic chemistry
License:
This work is licensed under a CC BY-NC 3.0 License. Read Full License
N,N’–bis–(2,4,6–trimethylphenylamino)ethane dihydrobromide is obtained in a single step through the dialkylation of dibromoethane. It serves as a versatile starting material for the synthesis of imidazolium salts: SIMes.HBr, SIMes.HCl, SIMes.HPF6 and SIMes.HBF4.
Associated Publications
Synthesis of 1,2 diamines under environmentally benign conditions: application for the preparation of imidazolidiniums
by Stéphane P. Roche, Marie-Laure Teyssot, and Arnaud Gautier
Tetrahedron Letters (27 September, 2012)